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Volume : VI, Issue : II, March - 2016

GROWTH AND CHARACTERIZATION OF SULFANILAMIDE DOPED DIHYDROGEN HEXAFLUOROSILICATECRYSTAL

N. Mala ., C. Muthuselvi,B. Ravikumar and S. Pandiarajan .

By : Laxmi Book Publication

Abstract :

Single crystals of sulfanilamide doped dihydrogen hexafluorosilicate were grown by slow evaporation method at the room temperature. The grown crystals are characterized by the powder XRD, FT-IR, FT-Raman, UV-Visible spectroscopy and SEM studies. The powder XRD, FT–IR and FT–Raman studies reveal the presence of dihydrogen hexafluorosilicate with the drug compound of sulfanilamide in the complex form. The optical properties of the title compound were analyzed by using the UV-Visible spectroscopy. The surface morphology of the complex crystal was analyzed from the SEM microphotograph.

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    Cite This Article :

    N. Mala ., C. Muthuselvi,B. Ravikumar and S. Pandiarajan .(2016). GROWTH AND CHARACTERIZATION OF SULFANILAMIDE DOPED DIHYDROGEN HEXAFLUOROSILICATECRYSTAL. Indian Streams Research Journal, Vol. VI, Issue. II, http://isrj.org/UploadedData/7892.pdf

    References :

    1. M. Madigan, J. Martinko, D. Stahl, D. Clark, Brock Biology of Microorganisms (13th ed.), Pearson Education, (2012) 797.
    2. C.T. Supuran , A. Casini , A. Scozzafava, Development of sulfonamide carbonicanhydrase inhibitors, CRC Press; Boca Raton (FL),USA, (2004) 67.
    3. A.F. Hollemann, E. Wiberg, Hollemann-Wiberg, Lehrbuch der AnorganischenChemie, Vol. 102, 34 ed., Berlin; New York, (2007).
    4. C. Topacli, A. Topacli, Journal of Molecular Structure, 644 (2003) 145.
    5. H. T. Varghese, C. Y. Panicker, D. Philip, Spectrochim. Acta A. 65 (2006) 155.
    6. H. Tanak, K. Pawlus, M. K. Marchewka, A. Pietraszko, Spectrochim. Acta A: Molecular and Biomolecular Spectroscopy, 118 (2014) 82.
    7. M. Madigan, J. Martinko, D. Stahl, D. Clark, Brock Biology of Microorganisms (13th ed.), Pearson Education, (2012) 797.
    8. C.T. Supuran , A. Casini , A. Scozzafava, Development of sulfonamide carbonicanhydrase inhibitors, CRC Press; Boca Raton (FL),USA, (2004) 67.
    9. A.F. Hollemann, E. Wiberg, Hollemann-Wiberg, Lehrbuch der AnorganischenChemie, Vol. 102, 34 ed., Berlin; New York, (2007).
    10. C. Topacli, A. Topacli, Journal of Molecular Structure, 644 (2003) 145.
    11. H. T. Varghese, C. Y. Panicker, D. Philip, Spectrochim. Acta A. 65 (2006) 155.
    12. H. Tanak, K. Pawlus, M. K. Marchewka, A. Pietraszko, Spectrochim. Acta A: Molecular and Biomolecular Spectroscopy, 118 (2014) 82.
    13. Casini , A. Scozzafava, C.T. Supuran, Expert Opin. Ther.Patents 12 (2002) 1307.
    14. R.E. Smith, M. Ashiya, Nat. Rev. Drug. Discov., 6 (2007) 597.
    15. C.C. Brackett, H. Singh, J.H. Block, Pharmacotherapy, 24 (2004) 856.
    16. P.G. Roegers, A Guide to the Complete Interperation of Infrared Spectra of Organic Structures, Wiley, Canada, (1994).
    17. Topacli, B. Kesimli, Spectrosc. Lett.34 (2001) 513.
    18. Casini , A. Scozzafava, C.T. Supuran, Expert Opin. Ther.Patents 12 (2002) 1307.
    19. M. Madigan, J. Martinko, D. Stahl, D. Clark, Brock Biology of Microorganisms (13th ed.), Pearson Education, (2012) 797.
    20. C.T. Supuran , A. Casini , A. Scozzafava, Development of sulfonamide carbonicanhydrase inhibitors, CRC Press; Boca Raton (FL),USA, (2004) 67.
    21. A.F. Hollemann, E. Wiberg, Hollemann-Wiberg, Lehrbuch der AnorganischenChemie, Vol. 102, 34 ed., Berlin; New York, (2007).
    22. C. Topacli, A. Topacli, Journal of Molecular Structure, 644 (2003) 145.
    23. H. T. Varghese, C. Y. Panicker, D. Philip, Spectrochim. Acta A. 65 (2006) 155.
    24. H. Tanak, K. Pawlus, M. K. Marchewka, A. Pietraszko, Spectrochim. Acta A: Molecular and Biomolecular Spectroscopy, 118 (2014) 82.
    25. Casini , A. Scozzafava, C.T. Supuran, Expert Opin. Ther.Patents 12 (2002) 1307.
    26. P. A. Ajibade, G.A. Kolawole, P. O’Brien, M. Helliwell, J. Raftery, Inorg. Chim.Acta. 359 (2006) 3111.
    27. P. A. Ajibade, G.A. Kolawole, P. O’Brien, M. Helliwell, J. Raftery, Inorg. Chim.Acta. 359 (2006) 3111.
    28. Casini , A. Scozzafava, C.T. Supuran, Expert Opin. Ther.Patents 12 (2002) 1307.
    29. R.E. Smith, M. Ashiya, Nat. Rev. Drug. Discov., 6 (2007) 597.
    30. C.C. Brackett, H. Singh, J.H. Block, Pharmacotherapy, 24 (2004) 856.
    31. P.G. Roegers, A Guide to the Complete Interperation of Infrared Spectra of Organic Structures, Wiley, Canada, (1994).
    32. Topacli, B. Kesimli, Spectrosc. Lett.34 (2001) 513.
    33. R.E. Smith, M. Ashiya, Nat. Rev. Drug. Discov., 6 (2007) 597.
    34. C.C. Brackett, H. Singh, J.H. Block, Pharmacotherapy, 24 (2004) 856.
    35. P.G. Roegers, A Guide to the Complete Interperation of Infrared Spectra of Organic Structures, Wiley, Canada, (1994).
    36. Topacli, B. Kesimli, Spectrosc. Lett.34 (2001) 513.
    37. Casini , A. Scozzafava, C.T. Supuran, Expert Opin. Ther.Patents 12 (2002) 1307.
    38. M. Madigan, J. Martinko, D. Stahl, D. Clark, Brock Biology of Microorganisms (13th ed.), Pearson Education, (2012) 797.
    39. C.T. Supuran , A. Casini , A. Scozzafava, Development of sulfonamide carbonicanhydrase inhibitors, CRC Press; Boca Raton (FL),USA, (2004) 67.
    40. A.F. Hollemann, E. Wiberg, Hollemann-Wiberg, Lehrbuch der AnorganischenChemie, Vol. 102, 34 ed., Berlin; New York, (2007).
    41. C. Topacli, A. Topacli, Journal of Molecular Structure, 644 (2003) 145.
    42. H. T. Varghese, C. Y. Panicker, D. Philip, Spectrochim. Acta A. 65 (2006) 155.
    43. H. Tanak, K. Pawlus, M. K. Marchewka, A. Pietraszko, Spectrochim. Acta A: Molecular and Biomolecular Spectroscopy, 118 (2014) 82.
    44. R.E. Smith, M. Ashiya, Nat. Rev. Drug. Discov., 6 (2007) 597.
    45. C.C. Brackett, H. Singh, J.H. Block, Pharmacotherapy, 24 (2004) 856.
    46. P.G. Roegers, A Guide to the Complete Interperation of Infrared Spectra of Organic Structures, Wiley, Canada, (1994).
    47. Topacli, B. Kesimli, Spectrosc. Lett.34 (2001) 513.
    48. R.E. Smith, M. Ashiya, Nat. Rev. Drug. Discov., 6 (2007) 597.
    49. C.C. Brackett, H. Singh, J.H. Block, Pharmacotherapy, 24 (2004) 856.
    50. P.G. Roegers, A Guide to the Complete Interperation of Infrared Spectra of Organic Structures, Wiley, Canada, (1994).
    51. Topacli, B. Kesimli, Spectrosc. Lett.34 (2001) 513.
    52. P. A. Ajibade, G.A. Kolawole, P. O’Brien, M. Helliwell, J. Raftery, Inorg. Chim.Acta. 359 (2006) 3111.
    53. M. Madigan, J. Martinko, D. Stahl, D. Clark, Brock Biology of Microorganisms (13th ed.), Pearson Education, (2012) 797.
    54. R.E. Smith, M. Ashiya, Nat. Rev. Drug. Discov., 6 (2007) 597.
    55. C.C. Brackett, H. Singh, J.H. Block, Pharmacotherapy, 24 (2004) 856.
    56. P.G. Roegers, A Guide to the Complete Interperation of Infrared Spectra of Organic Structures, Wiley, Canada, (1994).
    57. Topacli, B. Kesimli, Spectrosc. Lett.34 (2001) 513.
    58. C.T. Supuran , A. Casini , A. Scozzafava, Development of sulfonamide carbonicanhydrase inhibitors, CRC Press; Boca Raton (FL),USA, (2004) 67.
    59. A.F. Hollemann, E. Wiberg, Hollemann-Wiberg, Lehrbuch der AnorganischenChemie, Vol. 102, 34 ed., Berlin; New York, (2007).
    60. C. Topacli, A. Topacli, Journal of Molecular Structure, 644 (2003) 145.
    61. H. T. Varghese, C. Y. Panicker, D. Philip, Spectrochim. Acta A. 65 (2006) 155.
    62. H. Tanak, K. Pawlus, M. K. Marchewka, A. Pietraszko, Spectrochim. Acta A: Molecular and Biomolecular Spectroscopy, 118 (2014) 82.
    63. M. Madigan, J. Martinko, D. Stahl, D. Clark, Brock Biology of Microorganisms (13th ed.), Pearson Education, (2012) 797.
    64. C.T. Supuran , A. Casini , A. Scozzafava, Development of sulfonamide carbonicanhydrase inhibitors, CRC Press; Boca Raton (FL),USA, (2004) 67.
    65. A.F. Hollemann, E. Wiberg, Hollemann-Wiberg, Lehrbuch der AnorganischenChemie, Vol. 102, 34 ed., Berlin; New York, (2007).
    66. C. Topacli, A. Topacli, Journal of Molecular Structure, 644 (2003) 145.
    67. H. T. Varghese, C. Y. Panicker, D. Philip, Spectrochim. Acta A. 65 (2006) 155.
    68. H. Tanak, K. Pawlus, M. K. Marchewka, A. Pietraszko, Spectrochim. Acta A: Molecular and Biomolecular Spectroscopy, 118 (2014) 82.
    69. Casini , A. Scozzafava, C.T. Supuran, Expert Opin. Ther.Patents 12 (2002) 1307.
    70. P. A. Ajibade, G.A. Kolawole, P. O’Brien, M. Helliwell, J. Raftery, Inorg. Chim.Acta. 359 (2006) 3111.
    71. P. A. Ajibade, G.A. Kolawole, P. O’Brien, M. Helliwell, J. Raftery, Inorg. Chim.Acta. 359 (2006) 3111.
    72. P. A. Ajibade, G.A. Kolawole, P. O’Brien, M. Helliwell, J. Raftery, Inorg. Chim.Acta. 359 (2006) 3111.

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